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Following this intercomparison, a meeting was held in Turin in September-October 1986 at which seven radiocarbon laboratories (five AMS and two small gas-counter) recommended a protocol for dating the shroud. The samples were then taken to the adjacent Sala Capitolare where they were wrapped in aluminium foil and subsequently sealed inside numbered stainless-steel containers by the Archbishop of Turin and Dr Tite.In October 1987, the offers from three AMS laboratories (Arizona, Oxford and Zurich) were selected by the Archbishop of Turin, Pontifical Custodian of the shroud, acting on instructions from the Holy See, owner of the shroud. Samples weighing 50 mg from two of the three controls were similarly packaged.

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The three control samples, the approximate ages of which were made known to the laboratories, are listed below. T/32) from a tomb excavated at Qasr Ibrîm in Nubia by Professor J. This linen was dated in the British Museum Research Laboratory using liquid scintillation counting, giving a radiocarbon age of 2,010 ± 80 yr BP (BM-2558).

Two were in the form of whole pieces of cloth (samples 2 and 3) and one was in the form of threads (sample 4). This corresponds to a calendar age, rounded to the nearest 5 years, of 110 cal BC - AD 75 cal at the 68 per cent confidence level (where cal denotes calibrated radiocarbon dates). Threads removed from the cope of St Louis d'Anjou which is held in a chapel in the Basilica of Saint-Maximin, Var, France.

The second pair of subsamples was treated with a commercial detergent (1.5% SDS), distilled water, 0.1% HCL and another detergent (1.5% triton X-100); they were then submitted to a Soxhlet extraction with ethanol for 60 min and washed with distilled water at 70° C in an ultrasonic bath (method b).

The Oxford group divided the precleaned sample into three.

Testore of Department of Materials Science, Turin Polytechnic and G. If the samples had been unravelled or shredded rather than being given to the laboratories as whole pieces of cloth, then it would have been much more difficult, but not impossible, to distinguish the shroud sample from the controls.

Vial of Musée des Tissues and Centre International d'Étude des Textiles Anciens in Lyon), Dr M. Tite of the British Museum, representatives of the three radiocarbon-dating laboratories (Professor P. (With unravelled or shredded samples, pretreatment cleaning would have been more difficult and wasteful.) Because the shroud had been exposed to a wide range of potential sources of contamination and because of the uniqueness of the samples available, it was decided to abandon blind-test procedures in the interests of effective sample pretreatment.

Zurich precleaned the sample in an ultrasonic bath.

After these initial cleaning procedures, each laboratory split the samples for further treatment.

1 - Department of Geosciences, 2 - Department of Physics, University of Arizona, Tucson, Arizona 85721, USA 3 - Research Laboratory for Archaeology and History of Art, University of Oxford, Oxford, OX1 3QJ, UK 4 - Institut für Mittelenergiephysik, ETH-Hönggerberg, CH-8093 Zürich, Switzerland 5 - Lamont-Doherty Geological Observatory, Columbia University, Palisades, New York 10964, USA 6 - Research Laboratory, British Museum, London WC1B 3DG, UK Very small samples from the Shroud of Turin have been dated by accelerator mass spectrometry in laboratories at Arizona, Oxford and Zurich.

As Controls, three samples whose ages had been determined independently were also dated.

But the three laboratories undertook not to compare results until after they had been transmitted to the British Museum.

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